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Substituent effects which indicate increased reactivity of aromatics with electrondonating substituents directing the incoming nitro group to the artha and para positions are additional strong evidence for an electrophilic mechanism The NOt ion was also identified and characterized by cryoscopic and spectroscopic studies68 ,69 and, subsequently, stable nitronium salts were prepared70 and employed56 in electrophilic nitration Studies with preformed nitronium salts led eventually to the establishment of a modified mechanism necessitating two intermediates Olah and coworkers studied the competitive nitration of benzene and alkylbenzenes with nitronium tetrafluoroborate71 ,72 and with other nitronium salts 71 ,73 They observed high positional selectivities (high artha/para substitution with minor amounts of the meta isomer) similar to those in nitration with nitric acid-sulfuric acid Substrate selectivities, namely, relative rates of nitration of alkylbenzenes versus benzene, were found to be close to unity, which is in sharp contrast to the results in the mixed acid. free code 39 font for word Code 39 Word Barcode Add-In. Free Download Word 2019/2016 ...
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